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RoHS 2.0 Phenylene Testing Pyrolysis Gas Chromatograph DX-6600M

RoHS 2.0 Phenylene Testing Pyrolysis Gas Chromatograph DX-6600M

17600.0 USD ($)/Piece

Product Details:

  • Gas Pressure Carrier gas pressure: 0.4-0.5 MPa (adjustable)
  • Port Size Standard gas chromatograph column interface size
  • Accuracy 3% FS or better (method dependent)
  • Application RoHS/ELV/WEEE compliance testing, environmental protection, electronic materials analysis
  • Hardness N/A (not a hardness-rated product)
  • Temperature Ambient +5C to 350C (oven); Maximum ramp rate: up to 30C/min
  • Specimen Size 5-50 mg (typical sample mass range for pyrolysis)
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RoHS 2.0 Phenylene Testing Pyrolysis Gas Chromatograph DX-6600M Price And Quantity

  • 17600.0 USD ($)/Piece
  • 1 Piece

RoHS 2.0 Phenylene Testing Pyrolysis Gas Chromatograph DX-6600M Product Specifications

  • Touchscreen panel / PC Software control
  • Carrier gas pressure: 0.4-0.5 MPa (adjustable)
  • Single sample tube per analysis (autosampler optional)
  • Standard gas chromatograph column interface size
  • 3% FS or better (method dependent)
  • Programmable, adjustable as per analysis requirements
  • N/A (not a hardness-rated product)
  • RoHS/ELV/WEEE compliance testing, environmental protection, electronic materials analysis
  • 5-50 mg (typical sample mass range for pyrolysis)
  • Ambient +5C to 350C (oven); Maximum ramp rate: up to 30C/min
  • 80% RH, non-condensing
  • 0.01 ppm or better (method and detector dependent)
  • 50/60 Hz
  • N/A (not applicable for GC instruments)
  • AC 220V, 50/60Hz
  • 7-inch TFT touchscreen LCD
  • USB, RS232, LAN Ethernet
  • 0.01 ppm - 1000 ppm (method dependent)
  • <1 second (detector), method-dependent for full analysis
  • RoHS 2.0 analytes (phthalates, PBDE, PBB, and others as required)
  • Semi-automatic (fully automatic with autosampler)
  • Approximately 45 kg
  • Single sample per run (multiple runs possible with autosampler)
  • Approx. 450 mm
  • 220V AC
  • High temperature pyrolysis interface, multiple detection modes, system self-diagnosis, real-time data acquisition, user-friendly interface
  • Pyrolysis Gas Chromatograph for RoHS 2.0 Phenylene Testing
  • Analytical laboratory, compliance testing, research institutes
  • Benchtop/Laboratory Setup
  • Internal data storage or external export via USB
  • 610 510 450 mm
  • Ambient to 1000C (configurable)
  • 22 L
  • Windows 7/10 compatible analysis and reporting software
  • Automatic gas shutoff, over-temperature protection, leak detection
  • FID (Flame Ionization Detector) standard; other detectors optional
  • Hydrogen, Nitrogen, Helium (user selectable)

Product Description

1. Product Overview

RoHS is the European Union's legislation restricting the use of hazardous substances in electrical and electronic equipment (EEE). Its full name is the "Restriction of Hazardous Substances Directive." This directive primarily regulates the material and process standards of electrical and electronic products, making them more beneficial to human health and the environment. Initially, the directive established limits for the use of six substances in electrical and electronic products: lead, mercury, cadmium, hexavalent chromium, polybrominated biphenyls, and polybrominated diphenyl ethers. On June 4, 2015, the Official Journal of the European Union (OJ) published the revised RoHS 2.0 Directive (EU) 2015/863, officially adding DEHP, BBP, DBP, and DIBP to the list of restricted substances. Following the publication of this revised directive, EU member states were required to transpose and implement it in their respective national regulations by December 31, 2016. Furthermore, starting July 22, 2019, all electrical and electronic products (except medical and monitoring equipment) exported to the EU will be required to comply with these restrictions. Starting July 22, 2021, medical devices (including in vitro medical devices) and monitoring equipment (including industrial monitoring equipment) will also be subject to these restrictions.

Testing for the four phthalate esters in electrical and electronic products requires pulverizing, extracting, cleaning, and contaminating the electronic samples before testing with the appropriate instruments. This initial sample preparation is time-consuming. In March 2017, the Py/TD-GC-MS method was officially approved by the International Electrotechnical Commission (IEC) (a national standard has also been established, pending approval). This method is used to analyze phthalates restricted by the RoHS Directive (IEC 62321-8:2017) for the regulation of electrical and electronic products. As a low-profile alternative to Py/TD-GC-MS, Py/TD-GC has been extensively tested and shown to generally meet the RoHS 2.0 phthalate screening requirements.

Compared to traditional Soxhlet extraction, the Py/TD-GC coupled system allows for rapid screening of phthalates in electrical and electronic products. This method requires no pretreatment and eliminates the need for organic solvents. Results can be obtained directly from weighed samples, making it simpler and faster.

2. Applications

Four phthalates in polymers regulated by RoHS 2.0

3. Features

3.1 Rapid screening, professional software, and simple operation;

3.2 Temperature control utilizes a programmed temperature ramp design;

3.3 Equipped with a heat dissipation system, the instrument reduces instrument setup time and improves testing efficiency;

3.4 No cold spots during injection, ensuring repeatability and accuracy;

3.5 No organic solvents are required for sample preparation;

3.6 Compatible with a variety of sample matrices (liquid, solid, powder, etc.);

3.7 GC temperature and pressure control precision reaches best-in-class levels, ensuring excellent test repeatability;

3.8 Strong scalability meets the analysis needs of complex samples;

3.9 The instrument software automatically processes data, and analysis results reports are automatically generated upon test completion;

3.10 Simple installation and operation, compact footprint, high overall performance, and a competitive price.

4 .Instrument Technical Parameters and Specifications

Item

Performance Specifications

Inlet Type

Split/Splitless Pyrolysis Inlet

Inlet Temperature Range

100C to 400C above ambient temperature

Flame Ionization Detector Detection Limit

110-11 g/s (n-hexadecane/isooctane)

Column Oven Temperature

3C to 400C above ambient temperature;

Accuracy: 0.1C

Heating Rate: 0.1-40C/min, in 0.1C/min increments. Cooling Rate: Column chamber from 250C to 50C, no more than 8 minutes.

Temperature Program Repeatability: no more than 1%.

Initial and Final Temperature Time: 0.1-256 minutes.

Other Features

The instrument utilizes a multi-processor parallel operation mode, making it more stable and reliable. A variety of high-performance detectors are available, including FID, TCD, ECD, FPD, and NPD. Up to three detectors can be installed simultaneously. The FID detector has an auto-ignition function.

5. Analysis

5.1 Analysis Process

(I) Sample Preparation

Weigh the sample to a total mass of 0.5-1.0 mg. Weigh the sample boat and return the balance to zero. Use a carving knife to cut approximately 0.5 mg of sample and place it in the sample cup. Then, place the sample tube in the heating device.

(II) Reference Conditions

1) Sample Split Injection: Solid sample weight should be between 0.5 mg and 1 mg, liquid sample weight should be approximately 1 l

2) FID detector temperature: 300C, injection port temperature: 300C

3) Temperature program: 100C (hold for 1 minute), then increase at 20C/min to 300C (hold for 14 minutes)



Precision Testing for RoHS 2.0 Compliance

The DX-6600M is specially designed to facilitate high-accuracy testing of hazardous substances regulated under RoHS 2.0, including phthalates, PBDEs, and PBBs. Its advanced detection and pyrolysis capabilities provide rapid and reliable data critical for regulatory compliance in electronics manufacturing and environmental monitoring.


Advanced User Interface and Software Integration

The instrument features a 7-inch TFT touchscreen LCD and Windows 7/10 compatible software, allowing seamless control, real-time monitoring, and comprehensive reporting. These features support both novice and experienced users, making data handling and method programming convenient and efficient.


Enhanced Safety and Automation Features

Safety and operational efficiency are prioritized with automatic gas shutoff, over-temperature protection, and leak detection. The DX-6600M's semi-automatic setup can be fully automated with an autosampler, enabling high throughput and reducing user intervention while maintaining robust self-diagnostic protocols.

FAQ's of RoHS 2.0 Phenylene Testing Pyrolysis Gas Chromatograph DX-6600M:


Q: How does the DX-6600M Gas Chromatograph ensure compliance with RoHS 2.0 standards?

A: The DX-6600M is engineered to accurately detect and quantify hazardous substances such as phthalates, PBDEs, and PBBs as required by RoHS 2.0. It utilizes advanced pyrolysis and sensitive detector options, supporting precisely controlled analysis methods that meet regulatory requirements.

Q: What is the process for conducting a typical analysis with the DX-6600M?

A: To conduct an analysis, a prepared sample (typically 5-50 mg) is loaded into the pyrolysis interface and heated to target temperatures (up to 1000C as configured). The decomposed vapors are then separated in the GC column and detected, with results visualized and stored or exported via user-friendly software.

Q: Where can the DX-6600M be used most effectively?

A: This instrument is ideal for analytical laboratories, compliance testing centers, research institutes, and quality assurance departments. Its robust design and flexible automation features accommodate rigorous sample loads and evolving analytical needs.

Q: When should I consider using the autosampler option with this chromatograph?

A: An autosampler is recommended for high-throughput or repetitive analyses, as it automates sample introduction and increases operational efficiency. For single run analyses, manual loading suffices, but productivity is notably improved with automated sample handling in larger testing scenarios.

Q: What are the benefits of the touchscreen LCD and compatible software?

A: The 7-inch touchscreen LCD provides intuitive instrument operation, allowing real-time control and status monitoring. The included analysis and reporting software (Windows 7/10 compatible) streamlines data management, report generation, and facilitates integration into existing laboratory workflows.

Q: How does the DX-6600M ensure safe and efficient operation?

A: Safety is enforced through automatic gas shutoff, over-temperature protection, and integrated leak detection. Additionally, the system offers real-time self-diagnostics and can be monitored or controlled remotely, minimizing risks and enhancing laboratory safety standards.

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